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A D V A N C E D

M A T E R I A L S

&

P R O C E S S E S |

M A Y

2 0 1 6

3 9

the microstructure with orientation

information. The method has been

used on Ti, Ni, Zr, and Al alloys.

Researchers at The Ohio State

University, Columbus, are using STEM

to characterize the

α

/

β

interface in

three different types of

α

precipitates

in Ti-5Al-5V-5Mo-3Cr. High-angle annu-

lar dark-field (HAADF) imaging iden-

tifies and quantifies the terrace and

ledge structure along the

α

/

β

inter-

face. This provides valuable insight

into the influence of the

α

/

β

interface

on mechanical properties, which can

be used to develop predictive models

to optimize processing. Microtextured

regions (MTRs) have a deleterious effect

on dwell fatigue response for various

near

α

and

α

+

β

titanium alloys. Robust

microtexture characterization meth-

ods that include size, hard/soft grain

orientations, and misorientations were

developed.

One method uses DREAM-3D

(Hampshire, UK) open-source soft-

ware to extract critical MTR metrics

from representative samples. Data is

used to create statistically equivalent

synthetic microstructures to assess

the probability of certain microtexture

combinations that could manifest a

given volume of material (Fig. 3). After

identifying critical microstructure and

texture combinations, synthetic vol-

ume elements created in DREAM-3D are

analyzed in a finite element analysis

package with a linked crystal-plasticity

code to assess damage accumulation.

Overall, the conference was well

received with technical discussions

in just about every technology area

including extraction, melting, thermo-

mechanical processing, machining,

welding, additive manufacturing, and

more. All countries active in the tita-

nium industry were well represented.

Note: TIMETAL54M and ATI 425

are registered trademarks of Timet and

Allegheny Technologies Inc., respec-

tively. RTI-XPT is a trademark of RTI

International Metals Inc. CermeTi-10

is a registered trademark of Dynamet

Technology Inc.

~AM&P

References

1.

www.titanium.org/?page=Technical- Library

ITA 2014 Proceedings, ITA 2014

Proceedings.

Fig. 3 —

Synthetic volume element created in DREAM-3D.

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